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Alov N. V., Oskolok K. V.
Electron-Probe X-Ray
Microanalysis of the Electrochemically Modified Surfaces of Solid Disc
Electrodes
Abstract
The technique of electron-probe X-ray microanalysis
of surfaces of solid disc electrodes with different radii electrochemically
modified during metal and alloy deposition was developed. This technique allows
to study an element distribution along electrode surface and to estimate its
total content. The efficiency of proposed technique was tested during state
diagnostics of glass-ceramic carbon electrode surfaces after electrodeposition
of copper, cadmium and lead from aqueous solutions under different conditions.
The results of X-ray microanalysis were shown correlating to the conclusions of
theoretic electrochemistry.
Copyright (C) Chemistry Dept., Moscow State University, 2002
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